Magritek Spinsolve 60
- Resolution: <0.5 Hz (50%) / <20 Hz (0.55%)
- Sensitivity: 130:1 for 1% ethylbenzene
- 3D PFG gradients optimised for gradient-enhanced methods
- No cryogenic gases necessary
- External hardware lock, deuterated solvents not required
- WET solvent suppression
- Suitable for online reaction monitoring
- Simple operation
Experiments:
1H | 1H | 1D proton |
1H{¹⁹F} | 1D proton fluorine decoupled | |
1H{³¹P} | 1D proton phosphorous decoupled | |
1H WET SUP | 1D proton WET solvent suppression (of up to three solvent peaks, weighted by the T₁ relaxation) | |
1H WET T₂ | 1D proton WET solvent suppression (weighted by the T₂ relaxation time) | |
1H¹H COSY WET SUP | 2D COSY WET solvent suppression (of up to three solvent peaks) | |
1H param. | 1D proton wider chemical shift spread & shorter relaxation times | |
1H¹H COSY | 2D proton correlation spectroscopy | |
1H¹H TOCSY | 2D total correlated spectroscopy | |
1H¹H ROESY | 2D rotating frame overhauser enhancement spectroscopy | |
1H Jres | 2D homonuclear J-resolved spectrum | |
T₁ | measurement of T₁ relaxation times | |
T₂ | measurement of T₂ relaxation times | |
19F | 19F | 1D fluorine |
19F{¹H} | 1D fluorine proton decoupled | |
19F{³¹P} | 1D fluorine phosphorous decoupled | |
19F¹⁹F COSY | 2D fluorine correlation spectroscopy | |
19F Jres | 2D homonuclear J-resolved spectrum | |
1H¹⁹F COSY | 2D heteronuclear correlation spectroscopy | |
T₁ | measurement of T₁ relaxation times | |
T₂ | measurement of T₂ relaxation times | |
31P | 31P | 1D phosphorous |
31P{¹H} | 1D proton proton decoupled | |
1H³¹P HMBC | 2D heteronuclear multiple bond correlation | |
T₁ | measurement of T₁ relaxation times |