Magritek Spinsolve 60
Magritek Spinsolve 60
- Resolution: <0.5 Hz (50%) / <20 Hz (0.55%)
- Sensitivity: 130:1 for 1% ethylbenzene
- 3D PFG gradients optimised for gradient-enhanced methods
- No cryogenic gases required
- External hardware lock, deuterated solvents not required
- WET solvent suppression
- Suitable for online reaction monitoring
- Simple operation
Experiments:
| ¹H: | ¹H | 1D proton |
| ¹H{¹⁹F} | 1D proton fluorine decoupled | |
| ¹H{³¹P} | 1D proton phosphorus decoupled | |
| ¹H WET SUP | 1D proton WET solvent suppression (of up to three solvent peaks, weighted by the T₁ relaxation) | |
| ¹H WET T₂ | 1D proton WET solvent suppression (weighted by the T₂ relaxation time) | |
| ¹H¹H COSY WET SUP | 2D COSY WET solvent suppression (of up to three solvent peaks) | |
| ¹H param. | 1D proton wider chemical shift spread & shorter relaxation times | |
| ¹H¹H COSY | 2D proton correlation spectroscopy | |
| ¹H¹H TOCSY | 2D proton total correlation spectroscopy | |
| ¹H¹H ROESY | 2D rotating frame overhauser enhancement spectroscopy | |
| ¹H Jres | 2D homonuclear J-resolved spectrum | |
| T₁ | measurement of the T₁ relaxation times | |
| T₂ | measurement of the T₂ relaxation times | |
| ¹⁹F: | ¹⁹F | 1D fluorine |
| ¹⁹F{¹H} | 1D fluorine proton decoupled | |
| ¹⁹F{³¹P} | 1D fluorine phosphorus decoupled | |
| ¹⁹F¹⁹F COSY | 2D fluorine correlation spectroscopy | |
| ¹⁹F Jres | 2D homonuclear J-resolved spectrum | |
| ¹H¹⁹F COSY | 2D heteronuclear correlation spectroscopy | |
| T₁ | measurement of the T₁ relaxation times | |
| T₂ | measurement of the T₂ relaxation times | |
| ³¹P | ³¹P | 1D phosphorus |
| ³¹P{¹H} | 1D phosphorus proton decoupled | |
| ¹H³¹P HMBC | 2D heteronuclear multiple bond correlation | |
| T₁ | measurement of the T₁ relaxation times | |