BRUKER Fourier 300
BRUKER Fourier 300
Fourier console in operation since May 2013 - Cryomagnet from 1987
Probe: DUL 13C-1H/D Z-GRD
Dual configuration
; the ¹H and ¹³C nuclei are fixed
; no other heteronuclei are available
Temperature experiments are not possible.
The Fourier 300 is in use during the day for ¹H measurements. All other experiments are carried out between
8 pm and 7 am. (Night-time measurements)
Experiments:
| ¹H: | ¹H | |
| ¹H_D1-120s | → d1 (relaxation time) = 120s | |
| ¹H¹H COSY | H–H correlation within a spin system | |
| ¹H¹H NOESY | H–H correlation due to spatial proximity | |
| ¹³C: | ¹³C{¹H} | |
| ¹³C{¹H} dept135 | CH₃/CH positive – CH₂ negative | |
| ¹³C{¹H} dept90 | CH-positive | |
| ¹H¹³C HMQC | ||
| ¹H¹³C HMBC | ||