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Leitung
Wissenschaftliche Leitung
Mitarbeiter
Magritek Spinsolve 60
- Auflösung: <0.5 Hz (50%) / <20 Hz (0.55%)
- Sensitivität: 130:1 für 1% Ethylbenzol
- 3D PFG Gradienten optimiert für Gradienten-verstärkte Methoden
- Keine kryogenen Gase notwendig
- Externer Hardware-Lock, deuterierte Lösungsmittel nicht nötig
- WET Lösungsmittelunterdrückung
- Geeignet für die Online-Reaktionsüberwachung
- Einfache Bedienung
Experimente:
1H | 1H | 1D proton |
1H{19F} | 1D proton fluorine decoupled | |
1H{31P} | 1D proton phosphorous decoupled | |
1H WET SUP | 1D proton WET solvent suppression (of up to three solvent peaks, weighted by the T1 relaxation) | |
1H WET T2 | 1D proton WET solvent suppression (weighted by the T2 relaxation time) | |
1H1H COSY WET SUP | 2D COSY WET solvent suppression (of up to three solvent peaks) | |
1H param. | 1D proton wider chemical shift spread & shorter relaxation times | |
1H1H COSY | 2D proton correlation spectroscopy | |
1H1H TOCSY | 2D total correlated spectroscopy | |
1H1H ROESY | 2D rotating frame overhauser enhancement spectroscopy | |
1H Jres | 2D homonuclear J-resolved spectrum | |
T1 | measurement of T1 relaxation times | |
T2 | measurement of T2 relaxation times | |
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19F | 19F | 1D fluorine |
19F{1H} | 1D fluorine proton decoupled | |
19F{31P} | 1D fluorine phosphorous decoupled | |
19F19F COSY | 2D fluorine correlation spectroscopy | |
19F Jres | 2D homonuclear J-resolved spectrum | |
1H19F COSY | 2D heteronuclear correlation spectroscopy | |
T1 | measurement of T1 relaxation times | |
T2 | measurement of T2 relaxation times | |
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31P | 31P | 1D phosphorous |
31P{1H} | 1D proton proton decoupled | |
1H31P HMBC | 2D heteronuclear multiple bond correlation | |
T1 | measurement of T1 relaxation times |