Kontakt

Leitung

Prof. Dr. Thomas Müller

 +49 (0) 441 798-3874

 W3 3-338
 

Wissenschaftliche Leitung

 +49 (0) 441 798-3657

 W3 3-353

Mitarbeiter


+49 (0) 441 798-3733

+49 (0) 441 798-3733

 +49 (0) 441 798-3733

 W3 0-184
 

Magritek Spinsolve 60

  • Auflösung: <0.5 Hz (50%) / <20 Hz (0.55%)
  • Sensitivität: 130:1 für 1% Ethylbenzol
  • 3D PFG Gradienten optimiert für Gradienten-verstärkte Methoden
  • Keine kryogenen Gase notwendig
  • Externer Hardware-Lock, deuterierte Lösungsmittel nicht nötig
  • WET Lösungsmittelunterdrückung 
  • Geeignet für die Online-Reaktionsüberwachung
  • Einfache Bedienung

 

Experimente:

1H

1H

1D proton

1H{19F}

1D proton fluorine decoupled

1H{31P}

1D proton phosphorous decoupled

1H WET SUP

1D proton WET solvent suppression (of up to three solvent peaks, weighted by the T1 relaxation)

1H WET T2

1D proton WET solvent suppression (weighted by the T2 relaxation time)

1H1H COSY WET SUP

2D COSY WET solvent suppression (of up to three solvent peaks)

1H param.

1D proton wider chemical shift spread & shorter relaxation times

1H1H COSY

2D proton correlation spectroscopy

1H1H TOCSY

2D total correlated spectroscopy

1H1H ROESY

2D rotating frame overhauser enhancement spectroscopy

1H Jres

2D homonuclear J-resolved spectrum

T1

measurement of T1 relaxation times

T2

measurement of T2 relaxation times

 

 

 

19F

19F

1D fluorine

19F{1H}

1D fluorine proton decoupled

19F{31P}

1D fluorine phosphorous decoupled

19F19F COSY

2D fluorine correlation spectroscopy

19F Jres

2D homonuclear J-resolved spectrum

1H19F COSY

2D heteronuclear correlation spectroscopy

T1

measurement of T1 relaxation times

T2

measurement of T2 relaxation times

 

 

 

31P

31P

1D phosphorous

31P{1H}

1D proton proton decoupled

1H31P HMBC

2D heteronuclear multiple bond correlation

T1

measurement of T1 relaxation times

(Stand: 08.07.2024)  | 
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